Skip to content

Evaluation of Mechanical and Microstructural Properties of Sustainable 3D-Printed Engineered Cementitious Composites Incorporating Hybrid PE/PVA Fibers and Yellow River Sand (2025-11)

10.1016/j.cscm.2025.e05578

Raza Ali, Tan Binglin, Jiajia Zhou, Umar Muhammad, Ali Syed, Iqbal Safdar, Yuan Chengfang
Journal Article - Case Studies in Construction Materials, No. e05578

Abstract

3D printing of cementitious composites is an emerging construction method that eliminates the reliance on steel reinforcement, thereby improving crack resistance. This study investigates the mechanical and microstructural properties of 3D-printed engineered cementitious composites (3DP-ECC) incorporating hybrid polyethylene (PE) and polyvinyl alcohol (PVA) fibers, along with Yellow River Sand (YRS) as a sustainable alternative to quartz sand. The utilization of the YRS lowers the cost of ECC production and addresses environmental concerns, such as sedimentation and flooding. Mechanical properties of 3DP-ECC were determined in the X, Y, and Z printing directions and compared to Cast specimens to determine anisotropic behaviour through Digital Image Correlation (DIC). X-ray Computed Tomography (XCT) and Scanning Electron Microscopy (SEM-EDS) were used to investigate the microstructural characteristics. Results show that the Cast and 3DP-ECC specimens exhibited strain-hardening with tensile strains exceeding 3%. At R25, the tensile strength results for Cast ECC and 3DP-ECC were 6.58 MPa and 4.60 MPa, respectively, while the tensile strain value was 4.60% and 3.90%, respectively. The four-point bending results show that the Cast and 3DP-ECC specimens in the Z-direction exhibited enhanced bending capacity and minor cracking, whereas the X- and Y-direction specimens showed 13% and 16% reductions, respectively, compared to the Z-direction. In terms of compressive strength, the R50 group showed strengths of 49.7 MPa in Cast specimens and 45.9 MPa in 3DP specimens. Microstructural analysis identified dense hydration gels and strong fiber–matrix bonding, although XCT showed interlayer voids in 3DP-ECC, and porosity decreased with higher YRS content. This study has shown that hybrid PE/PVA fibers and YRS have the potential to enhance the sustainability and crack resistance of 3DP-ECC. However, this study highlights the importance of maximizing fiber orientation and interlayer bonding to improve the structural performance of 3DP-ECC.

34 References

  1. Ali Muhammad, Qian Hui, Umar Muhammad, Fenglin Liu et al. (2025-10)
    Rheological, Mechanical, and Self-Recovery Performance of 3D-Printed ECC Reinforced with Shape Memory Alloy Fibers
  2. Aslani Farhad, Zhang Yifan (2024-06)
    Sustainable 3D Printed Concrete Structures Using High-Quality Secondary Raw Materials
  3. Bai Meiyan, Wu Yuching, Xiao Jianzhuang, Ding Tao et al. (2023-04)
    Workability and Hardened Properties of 3D Printed Engineered Cementitious Composites Incorporating Recycled Sand and PE-Fibers
  4. Bakhshi Amir, Zafar Muhammad, Hojati Maryam (2025-02)
    A Study on Achieving High Tensile Ductility in 3D-Printable Engineered Cementitious Composites Reinforced with 8mm Fibers
  5. Chen Kailun, Liu Qiong, Chen Bing, Zhang Shishun et al. (2024-01)
    A Review on Effect of Raw Materials on the Performance of 3D Printed Geopolymer System for Construction
  6. Chen Wenguang, Ye Junhong, Jiang Fangming, Fediuk Roman et al. (2024-05)
    Printability Region for 3D Printable Engineered Cementitious Composites
  7. Ding Tao, Xiao Jianzhuang, Zou Shuai, Yu Jiangtao (2021-03)
    Flexural Properties of 3D Printed Fiber-Reinforced Concrete with Recycled Sand
  8. Duan Jiaqi, Sun Shouzheng, Chi Shengfeng, Hu Chunyou et al. (2024-06)
    Effect of Process Parameters on Forming Quality and Flexural Strength of Continuous-Fiber-Reinforced Cement-Based 3D Printed Composites
  9. Jiang Youbau, Gao Pengxiang, Adhikari Sondipon, Yao Xiaofei et al. (2024-12)
    Studies on the Mechanical Properties of Inter-Layer Interlocking 3D Printed Concrete Based on a Novel Nozzle
  10. Jiang Youbau, Liu Yan, Zhang Zupan, Gao Pengxiang et al. (2025-03)
    Tensile Performance of Interlayer Interface of Interlocking 3D Printed Concrete with Single Toothlike Nozzle
  11. Khan Shoukat, İlcan Hüseyin, Aminipour Ehsan, Şahin Oğuzhan et al. (2023-07)
    Buildability-Analysis on Effect of Structural Design in 3D Concrete Printing:
    An Experimental and Numerical Study
  12. Khan Shoukat, Jassim Muhammad, İlcan Hüseyin, Şahin Oğuzhan et al. (2023-04)
    3D Printing of Circular Materials:
    Comparative Environmental Analysis of Materials and Construction Techniques
  13. Khan Mohammad, Sanchez Florence, Zhou Hongyu (2020-04)
    3D Printing of Concrete:
    Beyond Horizons
  14. Li Zhanzhao, Hojati Maryam, Wu Zhengyu, Piasente Jonathon et al. (2020-07)
    Fresh and Hardened Properties of Extrusion-Based 3D Printed Cementitious Materials:
    A Review
  15. Ma Guowei, Li Zhijian, Wang Li (2017-12)
    Printable Properties of Cementitious Material Containing Copper-Tailings for Extrusion-Based 3D Printing
  16. Ma Guowei, Li Zhijian, Wang Li, Wang Fang et al. (2019-01)
    Mechanical Anisotropy of Aligned Fiber-Reinforced Composite for Extrusion-Based 3D Printing
  17. Pan Zuanfeng, Si Doudou, Tao Jinghong, Xiao Jianzhuang (2023-02)
    Compressive Behavior of 3D Printed Concrete with Different Printing Paths and Concrete Ages
  18. Pang Zhiming, Lu Cong, Li Baoshan, Wang Jiajie (2023-02)
    A Multi-Scale Model for Quantifying Fiber-Orientation Effects on the Tensile Properties of 3D Printed Engineered Cementitious Composites
  19. Pi Yilin, Lu Cong, Li Baoshan, Zhou Junhui (2023-10)
    Crack Propagation and Failure Mechanism of 3D Printing Engineered Cementitious Composites (3DP-ECC) Under Bending Loads
  20. Raza Ali, Junjie Zhang, Fan Jiahui, Umar Muhammad et al. (2025-05)
    Comprehensive Study on the Microstructural and Mechanical Performance of 3D-Printed Engineered Cementitious Composites with Yellow River Sand Integration
  21. Rehman Atta, Melesse Birru, Kim Jung-Hoon (2023-02)
    Set-on-Demand 3D Concrete Printing Construction and Potential Outcome of Shotcrete-Accelerators on Its Hardened Properties
  22. Roussel Nicolas (2018-05)
    Rheological Requirements for Printable Concretes
  23. Sikora Paweł, Techman Mateusz, Federowicz Karol, Khayatt Ahmed et al. (2022-07)
    Insight into the Microstructural and Durability Characteristics of 3D Printed Concrete:
    Cast versus Printed Specimens
  24. Surehali Sahil, Tripathi Avinaya, Neithalath Narayanan (2023-08)
    Anisotropy in Additively Manufactured Concrete Specimens Under Compressive Loading:
    Quantification of the Effects of Layer-Height and Fiber-Reinforcement
  25. Varela Hugo, Barluenga Gonzalo, Sonebi Mohammed (2024-09)
    Evaluation of Basalt-Fibers and Nano-Clays to Enhance Extrudability and Buildability of 3D Printing Mortars
  26. Xiao Jianzhuang, Bai Meiyan, Wu Yuching, Duan Zhenhua et al. (2024-01)
    Inter-Layer Bonding Strength and Pore Characteristics of 3D Printed Engineered Cementitious Composites
  27. Xiao Jianzhuang, Han Nv, Zhang Lihai, Zou Shuai (2021-05)
    Mechanical and Microstructural Evolution of 3D Printed Concrete with Polyethylene-Fiber and Recycled Sand at Elevated Temperatures
  28. Ye Junhong, Cui Can, Yu Jiangtao, Yu Kequan et al. (2021-02)
    Effect of Polyethylene-Fiber Content on Workability and Mechanical-Anisotropic Properties of 3D Printed Ultra-High-Ductile Concrete
  29. Yu Kequan, McGee Wesley, Ng Tsz, Zhu He et al. (2021-02)
    3D Printable Engineered Cementitious Composites:
    Fresh and Hardened Properties
  30. Zhao Yu, Shen Guanghai, Zhu Lingli, Ding Yahong et al. (2025-06)
    Enhancing Interfacial Bonding and Pore Structure Optimization in 3D-Printed High-Strength ECC with Steel-PE Hybrid Fibers
  31. Zhou Wen, Zhang Yamei, Ma Lei, Li Victor (2022-04)
    Influence of Printing Parameters on 3D Printing Engineered Cementitious Composites
  32. Zhou Wen, Zhu He, Hu Wei-Hsiu, Wollaston Ryan et al. (2024-02)
    Low-Carbon, Expansive Engineered Cementitious Composites (ECC) In the Context of 3D Printing
  33. Zhu Binrong, Pan Jinlong, Li Junrui, Wang Penghui et al. (2022-07)
    Relationship Between Microstructure and Strain-Hardening Behavior of 3D Printed Engineered Cementitious Composites
  34. Zhu Binrong, Pan Jinlong, Zhou Zhenxin, Cai Jingming (2021-04)
    Mechanical Properties of Engineered Cementitious Composites Beams Fabricated by Extrusion-Based 3D

0 Citations

BibTeX
@article{raza_tan_jiaj_umar.2025.EoMaMPoS3PECCIHPPFaYRS,
  author            = "Ali Raza and Binglin Tan and Zhou Jiajia and Muhammad Umar and Syed Basit Ali and Safdar Iqbal and Chengfang Yuan",
  title             = "Evaluation of Mechanical and Microstructural Properties of Sustainable 3D-Printed Engineered Cementitious Composites Incorporating Hybrid PE/PVA Fibers and Yellow River Sand",
  doi               = "10.1016/j.cscm.2025.e05578",
  year              = "2025",
  journal           = "Case Studies in Construction Materials",
  pages             = "e05578",
}
Formatted Citation

A. Raza, “Evaluation of Mechanical and Microstructural Properties of Sustainable 3D-Printed Engineered Cementitious Composites Incorporating Hybrid PE/PVA Fibers and Yellow River Sand”, Case Studies in Construction Materials, p. e05578, 2025, doi: 10.1016/j.cscm.2025.e05578.

Raza, Ali, Binglin Tan, Zhou Jiajia, Muhammad Umar, Syed Basit Ali, Safdar Iqbal, and Chengfang Yuan. “Evaluation of Mechanical and Microstructural Properties of Sustainable 3D-Printed Engineered Cementitious Composites Incorporating Hybrid PE/PVA Fibers and Yellow River Sand”. Case Studies in Construction Materials, 2025, e05578. https://doi.org/10.1016/j.cscm.2025.e05578.